Proximate chemical composition of orange peel and variation of. The essential oils were analyzed by gas chromatography. Distillation is the most widely used method to produce essential oils. Therefore, the objective of this work was to determine the chemical composition and evaluate the toxicity of commercial sweet orange citrus sinensis, bitter orange citrus aurantium and sicilian lemon citrus limon essential oils and pure monoterpene dlimonene on d. Chemical composition of bitter orange essential oils.
Citrus peel, the primary waste, is a good source of molasses, pectin and limonene and is usually dried, mixed with dried pulps and sold as cattle feed bocco et al. The glycosides hesperidin and naringin are mainly responsible for the purported antioxidant activity of citrus peel extracts kanaze et al 2008. In particular the chemical composition of the cloud consists of 4. Antioxidant and anticancer activities of essential oil from. In the present study, an essential oil was prepared by cold pressing of gannan navel orange peel followed by molecular distillation.
Using gcms analysis, 11, 12 and 24 chemical constituents were identified in orange, lemon and lime essential oil respectively. A determination of some constituents of orange peels and studies its. Essential oil components of orange peels and antimicrobial activity. Proximate composition, total phenols and flavonoids of orange peel.
L was analysed by gas chromatographymass spectrometry gcms. International journal of environment agriculture and biotechnologyissn. Olabinjo and others published analysis of physical and chemical composition of sweet orange citrus sinensis peels find, read and cite all. In the present study we investigated the variation in the yield and chemical composition of the essential oils isolated from fresh. Analysis of physical and chemical composition of sweet orange citrus sinensis peels. The method is based on the initial treatment of the samples with dilute nitric acid to extract pectin according to the. Kulkarni2 1department of chemical engineering, visvesvaraya national institute of technology, nagpur 440 010, india 2csirnational chemical laboratory, pune 411 008, india globally, india is the leading producer of fruits. Orange peel definition of orange peel by merriamwebster. Orange oil is an essential oil produced by cells within the rind of an orange fruit citrus sinensis fruit. In view of previous findings, ascertaining the high antimi. This product has been classified in accordance with the hazard criteria of the cpr and the msds contains all the. Extraction and characterization of pectin from orange peels.
Chemical composition of citrus fruits orange, lemon, and grapefruit with respect to quality control of juice products. Chemical composition of citrus fruits orange, lemon, and. The chemical composition of the orange peel adsorbent as determined by xray fluorescence is shown in table 1. Orange rinds, proximate analysis, protein, crude fibre. Orange peel definition is a rough surface as on porcelain like that of an orange. Although, carrot peel accounted for only 11% of the amount of the carrot fresh weight, it could provide 54. It is composed of mostly greater than 90% dlimonene, and is often used in place of pure dlimonene. Agent orange active ingredients and characteristics. Unraveling the selective antibacterial activity and chemical. The chemical composition of the essential oil eo obtained by solvent. The chemical composition of the peel oils from unripe and ripe fruits.
Maltease orange peel is rich in nutritional ingredients such as soluble sugars 46. Peels of eight fresh fruits orange, watermelon, apple, pomegranate, pawpaw, banana, pineapple and mango were removed and analyzed for their nutrients and antinutrients contents. The main constituent of orange peel essential oil is dlimonene present to the extent of at least 90 %, which is the only hydrocarbon present 18, 19. In this study some physical and chemical properties of the primary waste of sweet orange was investigated. Characterization of the chemical composition of banana. Gannan in jiangxi province is the top navel orange producing area in china. Twenty four constituents were identified, representing 97. No significant differences were found in protein ash, and carbohydrate content of baladi and novel orange peel. In vitro digestibility and changes in the chemical composition of the fermented products were determined after seven days of fungal cultivation using gas production tests. It originated from southern china where it has been cultivated for many years, but is today grown commercially worldwide in. Chemical identifications of citrus peels essential oils.
All parts of an orange, including the seeds and leaves, are rich in vitamin c, which is a powerful antioxidant. Chemical composition and antimicrobial activity of leaf. Fiber in oranges helps prevent atherosclerosis and protects against rheumatoid arthritis. Citrus oils are a complex mixture of more than a hundred components of differing chemical natures. In contrast to most essential oils, it is extracted as a byproduct of orange juice production by centrifugation, producing a coldpressed oil. Orange peel waste was fermented with bacillus licheniformis shg10 to obtain. Chemistry and pharmacology of citrus sinensis mdpi. These results indicated that the samples tested were composed mainly of cellulose microfibrils containing hemicellulose and lignin 12, as shown in table 2. Chemical composition and antimicrobial activities of. Extraction and characterization of pectin from orange peels 43 plugged with a stopper and shaken vigorously, then allowed to stand at room temperature for 2 hours to deesterify pectin. No retention time active constituents quantity % 1 11. Phytochemical composition, antioxidant and antibacterial. Orange peel nutritional composition of orange peel.
In fact orange peel extract has been used in cancer studies for many years with no adverse effects 2. Under optimal conditions, 193 mg citric acidg dry orange peel was obtained torrado et al. Analysis and comparative study of essential oil extracted. Orange peel waste was fermented with bacillus licheniformis. Pe els of eight fresh fruits orange, watermelon, apple, pomegranate, pawpaw, banana, pineapple and mango were. Chemical composition of peel, leaf and flower essential oils. Pdf analysis of physical and chemical composition of sweet. Therefore, it is possible to obtain banana peel sufficiently and application depends on its chemical compositions. Chemical composition and protein enrichment of orange.
Volatile components of peel and leaf oils of lemon and lime. The results obtained in which the chemical composition of all decreased for example cl 36. Peel and leaf oils of 43 taxa of lemons and limes were obtained from fruits and leaves collected from trees submitted to the same pedoclimatic and cultural conditions. The chemical analysis showed sweet orange rinds to be rich in protein of 7. The result showed sweet orange rinds peels as the major waste and contains 4550% of the total mass of sweet orange fruits. Fifty constituents were quantified, comprising about 99% of the oils. Chemical composition and selected functional properties of. Dlimonene terpene is derived from the peels of citrus fruits, it is a cyclic monoterpene, patients use this supplement to prevent and treat cancer 23. This pamphlet is designed to explain the benefits of chemical peels, what to expect during the process and how to care for your skin after the treatment. All the nutritional information you need to know about orange peel can be found below. The study of the physiologically active components of citrics and their contribution to human health is a growing research field.
Chemical characterisation of the industrial residues of. Pdf analysis of physical and chemical composition of. Extraction of essential oil dlimonene from sweet orange peels by simple distillation ramgopal k, sreekanteshwara s, vijay bhaskar s a, vinodh s m, mr. Citrus peels orange and lemon peels were analysed for cellulose, hemicelluloses, acid insoluble lignin and ash using the method developed by aravantinosza. This research involves detection of the chemical constituents of orange peel. Chemical composition of the citrus limetta peel as analyzed by gcms2 s. It comes in several different varieties, including blood orange, navel oranges, valencia orange, clementine, and tangerine. Chemical composition of citrus fruits orange, lemon, and grapefruit with respect to quality control of juice products agnes sasskiss department of analytical chemistry, central food research institute, herman otto 15, 1022 budapest, hungary.
Orange peel extract is an allnatural product and its safety has been evaluated 21. Shukla, in fermented foods in health and disease prevention, 2017. The present experiment aimed at increasing orange peel and sugar beet pulp protein content through solidstate fermentation by trichoderma reesei and trichoderma viride. Orange juice is a suspension that consists of heterogeneous particles in a clear serum. Osbeck to dist inguish it from related closely species like sour orange, c. Volatile components of peel and leaf oils of lemon and. A determination of some constituents of orange peels and. Cellulose, hemicelluloses, lignin and ash content of some. Banana peel extract composition and method for extraction. Orange peel extract contains citrusderived polymethoxylated flavones that have an inhibitory effect on tnf. Yield and chemical composition of citrus essential oils as affected by drying pretreatment of peels abstract. Yield and chemical composition of citrus essential oils as affected by drying pretreatment of peels 1277 international food research journal 184.
Orange peel was shown to contain more amount of essential oil 20ml at 180minutes than lemon 7ml at 180minutes and lime 5ml at 180minutes. As well as variations in oranges used, some varieties include differing amounts of juice vesicles, known as pulp in american english, and juicy bits in. Essential oil composition and antibacterial activity of. Chemical composition, functional properties and processing of. Peels of banana were removed and analyzed for their nutrients and antinutrients contents. Chemical composition and antimicrobial activities of essential oil from the peel of bingtang sweet orange citrus sinensis osbeck. Analysis of physical and chemical composition of sweet orange. Mar 18, 2011 the phenolic contents in different tissues decreased in the following order peel phloem xylem.
Professor, department of chemical engineering, bms college of engineering, bangalore, india. Several types of chemical compounds have been identified in fruits. Analysis of physical and chemical composition of sweet. Orange essential oil is present in small ductless gland contained in the peel of the orange fruits. This study aims at investigating the chemical properties of the hexane and dichloromethane dcm extracts of orange peel as well as their biological potentials. Gst, and gsh after chemical induction of oxidative stress arafa et al 2009. Compounds found in orange peels helps lower cholesterol naturally. Extraction of essential oil dlimonene from sweet orange. Ripe bitter orange peels contained higher concentrations of aliphatic aldehydes and oxygencontaining. Their chemical composition was investigated by capillary gc, gcms, and c nmr, and the results were submitted to principal component analysis to check for chemical variability. Chemical characterization, antioxidant, antioxidative burst, and phytotoxic activities. The aim of this work was to determine the chemical composition of four citrus oils. Orange peel, which is the primary waste fraction in the production of orange juice, contains flavonoids associated with antioxidant activity kanaze et al 2008.
Orange peels were subjected to the production of citric acid by solidstate fermentation with aspergillus niger nrrl 599. Chemical composition and biological activities of lemon. The waste generated from the fruits needs to be put into a beneficial use. Chemical constituents were evaluated in terms of qualitative and quantitative analyses by gas chromatographymass spectrometry. Limonene is the main component of the citrus peel oils and it ranges from 4095% in concentration in citrus fruits. In addition, peels and seeds can present higher nutrient contents7. Sweet orange is one of the most common fruits in the world. It is composed of mostly greater than 90% dlimonene, and is often used in place of pure d. Chemical composition of peel, leaf and flower essential. Peel, pulp and peel fibre from citrus hystrix and citrus maxima red and white variety, could be used as potential dietary fibre sources in the enrichment of foods because of their high physicochemical properties. Maltease orange peel and to determine the effect of air temperature 40, 60, 80c on phenols and antioxidant activity kinetics of orange peel. Eating oranges may prevent ulcers and reduce the risk of stomach and colon. Chemical composition and antioxidant potential of peels from three varieties of banana. Percentage of important constituents in peel oils of some citrus fruits.
The peel fibre derived from orange fruit is involved in the improvement in intestinal function and health chau et al. Pummelo is a common citrus species in the country, thought to be the local version of grapefruit. Dietary fibre components and pectin chemical features of peels during ripening in. The chemical composition of bitter orange peel oils from fully developed, living, unripe and ripe fruits was studied. Orange juice is a liquid extract of the orange tree fruit, produced by squeezing or reaming oranges. The chemical compositions in orange peels used made it possible to use in herbal medicine for the treatment of many diseases 22. The flour samples were evaluated for proximate composition, mineralcontent and selected functional properties. The two active ingredients in the agent orange herbicide combination were equal amounts of 2,4dichlorophenoxyacetic acid 2,4d and 2,4,5trichlorophenoxyacetic acid 2,4,5t, which contained traces of 2,3,7,8tetrachlorodibenzopdioxin tcdd. Antioxidant and anticancer activities of essential oil. The monoterpenes and sesquiterpene hydrocarbons with 96. The result showed sweet orange rinds peels as the major waste and contains. Flour samples were prepared from dehulled and undehulledsweet orange citrus sinensis seeds. Its peels have been utilized for long as an active ingredient in most traditional medicines.
Pdf chemical composition of some selected fruit peels. The results showed that water content, crude protein contents, crude lipid contents, crude fiber, total ash contents and carbohydrate in banana peels were 50. The two active ingredients in the agent orange herbicide combination were equal amounts of 2,4dichlorophenoxyacetic acid 2,4d and 2,4,5trichlorophenoxyacetic acid 2,4,5t, which contained traces of. The chemical composition of the peel oils from unripe and. These results indicated that the samples tested were composed mainly of cellulose microfibrils containing hemicellulose and lignin 12, as shown in. Aug 22, 2017 gannan in jiangxi province is the top navel orange producing area in china. These uses will promote sustainable disposal of orange rinds.
Remember that results will vary and it is important to consult with a trained skin care professional before conducting a peel at home. Citrus peel essential oils have an impressive range of food and medicinal uses. This was due to rice husk briquettes as an absorber plate in the container of distilled lead compounds dissolved therein participate after. The chemical composition of the essential oil obtained from the peel of bingtang sweet orange citrus sinensis osbeck was analysed by gas chromatography and gas chromatographymass spectrometry gcms. Chemical characterisation of the industrial residues of the. The oils were chemically analysed and identified by gas chromatography mass spectrometry gcms. According to morais et al8 and moohuchin et al,9 peels are highly perishable, mainly due to the large amount of water in their composition.
All whmis required information is included in appropriate sections based on the ansi z400. Yield and chemical composition of citrus essential oils as. Characterization of the chemical composition of banana peels 323 and transferring it to 5mmnmr tubes. Each sample was collected from 10 fruits, mixed together, then cut into small pieces and used fresh for analysis or dried at 50ec for 48 h using air oven, the dried samples were ground to a fine powder and stored at 4ec for further analysis. There were 21 compounds in citrus essential oil where limonene 94. The unidimensional nmr spectra 1hnmr were recorded in a varian inova500 mhz nmr spectrometer and the chemical shifts. Lower aliphatic constituents are formed during ripening. Citrus peels are subdivided into the epicarp or flavedo coloured peripheral surface and mesocarp or albedo white soft middle layer as shown in fig.
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